Indirect Validity Test of Measurement Instrumentation in Flow Injection Synthesis Technique of Cu-Zn Ferrite Formation Process
Keywords:
, Flow Injection Synthesis (FIS), Non-Isothermal, Avrami methods, FIS Instrumentation, Reproducibility, Valid, Reliable, Data logger.Abstract
The Flow Injection Synthesis-FIS instrumentation measurement system has to validity test either will be used by workers or for the instrument validity test. Repeatability test is one of easy method to do indirect validity test. The test is done besides of the instrumentation data test but also product consistency test and production system. All of the measurements systems that will be tested have to fulfill requirement as valid and reliable measurement instrumentation. In this work six sample of X-Ray Diffraction test divided in two groups of temperature different have been prepared for repeatability test base in the yield of FIS process of Cu Zn Ferrite synthesis. All of the processes results have to validity test to convince the quantitative product analysis. The indirect test at six yields sample show high repeatability with atomic content deviations less than 2% but in relative validity, fulfill requirement product reproducibility workers. The FIS Instrumentation system include FIS reactor, pH data logger, peristaltic pump which its use in the non-isothermal reaction.
References
Sasito Edie.S.(2015) .,Synthesis and Determination of Cu-ZnFerrite Formation Energy Use Flow Injection Synthesis., Doctorate dissertation, University of Indonesia, Indonesia.
Willard M.A, Kurihara L.K, Carpenter E.E. Calvin S. Harris V.G., Chemically prepared magnetic nanoparticles., International Materials Reviews 2004 VOL 49, Published by Maney Publishing (c) IOM Communications L.
.Faraji,MY.Yamini* and M. Rezaee, Magnetic Nanoparticles:Synthesis,Stabilization,Functionalization, Charact and Appl, J. Iran. No. 1, March 2010, pp. 1-37., Tehran, Iran.
Ahmadi, Madaah hosseini and masoudi,2011,Avrami Behavior Of Magnetite Nanoparticles, Formation In Co-Precipitation Process, Dept of Mat Science and Engi, Sharif Univ Of Technology, Tehran, Iran.
Kaiser Robert, Rosenwig Ronald E, August 1969, STUDY OF FERROMAGNETIC LIQUID, AVCO CORPORATION, Lowell, Mass. For National Aeronautics And Space Admin Washington, D. C.
Alvarez G.S., Synthesis, Characterization, application Iron Oxide Nanoparticle, Doctoral thesis, stockolm- Sweden, 2004.
Sasito E, Soegijon B, Manaf A., Non-isothermal crystalliz Kinetic behav of Specific Cu(1-x)ZnxFerrite Formation in the Flow Injection Synthesis Co-precipt reactor., International Journal of Basic and Appl Sciences IJBAS-IJENS Vol 13 No 03.
Neil Ullman., What Are Repeatability And Reproducibility, Part 2: The E11 Viewpoint1., Magazines & Newsletters / Astm Standardization News.
Laurent S. at all, Magnetic Iron Oxide Nanoparticles: Synthesis, Stabilization, Vectorization, Physicochemical Charact, and Biological Appl., Chem. Rev. 2008, 108, 2064
Jena A.K. Chaturvedi M.C.,Phas Tranf in Material.,Prent Hall,Englewood Cliff, New Jersey,1992
Cherkezova.Z, Zeleva, 2011.,Std. of N.siz. Fer. Mat. Prep. by Co-Preci. Met.,In.of Cat.Bulg. Acad.of Sci, Sofia, Bulgaria, Sev. Nati. Conf. on Chemistry.
K.S.Lohar, S.M.Patange, Sagar E. Sirsath, V.S Surywanshi, S.S Gaikwad,Santosh SJadhav and Nilesh Kulkarni., Struc tRefin By Rietveld Method and Magnetic Study of Nano-Crystalline Cu-ZnFerrite., Int Jr of Adv in Eng &Technology, March 2012. ISSN:2231-1963.
Mohapatra* and S. Anand**, 2010 ,Synthesis and appl of nano-struct iron oxides/hydroxides
Doubelin E.O., Measurement Systems: Application and Design., Mc GRAW-HILL KOGAKUSHA,LTD.
Lohar K.S et all ., Structural Refin by Rietveld method and Magnetic Study of Nano-Cryst Cu-Zn Ferrites., Int Jr. of Adv in Engg and Techn-IJAET March 2012.
Nguyen T-D and Do Trong-On ., Size- and Shape-Controlled Synthesis of Monodisperse Metal Oxide and Mixed Oxide Nanocrystals., Dept of Chem. Engine., Laval University, Quebec Canada ,2011, www.intechopen.com.
Giri Jyotsnendu, Pradan Palab, Somani Vaibhav.,Synth and charact of water-based ferrofluid of substituted ferrite [ Fe1-xBxFe2O4, B=Mn,Co (x=0-1)] for biomedi. appl., Dept.of Mettal Engg and Mat. Sciences, Indian Institute of Techn, Mumbay, India.
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